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<title>UTas ePrints - Structural Studies of RSHg(II) Complexes Containing (-Hg-SR-)n Rings and Chains</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Raston, C.L." name="eprints.creators_name" />
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<meta content="Crystals of acetato(methanethio1ato)-gamma-picolinemercury(II), MeSHg02CMe,C6H7N (1), are monoclinic, P21/a, a 16.617(9), b 7.271(3), c 20.476(2), beta = 113.31(5), Z 8. The structure resembles that of its pyridine analogue, being based on a polymeric (-Hg-SMe-)n chain with acetate and
picoline groups coordinated at each mercury; a similar structure is found for EtSHg02CMe,C5H5N (2), monoclinic, P21/c, a 9.344(2), b 17.917(9), c 7.179(2) A, beta 106.24(3), Z 4. The structure of tetrachlorotetra(2-methylpropane-2-thiolato)di(gamma-picoline)tetramercury(11), (ButS)4CI4Hg4(C6H7N)2 (3), also resembles that of its pyridine analogue being based on an unusual tetranuclear grouping of mercury atoms linked by chloride and thiolate bridges. Crystals of (3) are monoclinic, P21/c
a 12.334(7), b 17.468(9), c 9.999(5) A, beta 91.18(4), Z 2. Crystals of MeSHgBr (4) are monolinic, P21/c, a 7.770(9), b 7.500(5), c 7.945(10) A, beta 91.71(3), Z 4, and contain parallel chains (-Hg-SMe-)n with neighbouring chains linked by bridging bromine atoms into parallel sheets. Each bromine is triply bridging, being coordinated to two mercury atoms in one chain, and one mercury atom in an adjacent chain. The structure of MeSHgCl appears to be isomorphous." name="eprints.abstract" />
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Canty, A. J., Kishimoto, R., and Tyson, R. K., Aust. J. Chem., 1978, 31, 671, and references
therein.
Puff, H., Sievers, R., and Elsner, G., 2. Anorg. Allg. Chem., 1975, 413, 37.
Canty, A. J., Raston, C. L., and White, A. H., Aust. J. Chem., 1978, 31, 677.
Carty, A. J., and Taylor, N. J., J. Am. Chem. Soc., 1977, 99, 6143.
Canty, A. J., and Tyson, R. K., Inorg. Chim. Acta, 1977, 24, L77.
Johansson, A., Ark. Kemi, Mineral. Geol., 1939, 13A, 1.
Cromer, D. T., and Mann, J. B., Acta Crystallogr., Sect. A, 1968, 24, 321.
Cromer, D. T., and Liberman, D., J. Chem. Phys., 1970, 63, 1691.
Stewart, R. F., Davidson, E. R., and Simpson, W. T., J. Chem. Phys., 1965, 42, 3175.
lo 'The X-RAY System-Version of March, 1976' Technical Report TR-446, Computer Sciencecenter,
University of Maryland, U.S.A." name="eprints.referencetext" />
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<meta content="Crystals of acetato(methanethio1ato)-gamma-picolinemercury(II), MeSHg02CMe,C6H7N (1), are monoclinic, P21/a, a 16.617(9), b 7.271(3), c 20.476(2), beta = 113.31(5), Z 8. The structure resembles that of its pyridine analogue, being based on a polymeric (-Hg-SMe-)n chain with acetate and
picoline groups coordinated at each mercury; a similar structure is found for EtSHg02CMe,C5H5N (2), monoclinic, P21/c, a 9.344(2), b 17.917(9), c 7.179(2) A, beta 106.24(3), Z 4. The structure of tetrachlorotetra(2-methylpropane-2-thiolato)di(gamma-picoline)tetramercury(11), (ButS)4CI4Hg4(C6H7N)2 (3), also resembles that of its pyridine analogue being based on an unusual tetranuclear grouping of mercury atoms linked by chloride and thiolate bridges. Crystals of (3) are monoclinic, P21/c
a 12.334(7), b 17.468(9), c 9.999(5) A, beta 91.18(4), Z 2. Crystals of MeSHgBr (4) are monolinic, P21/c, a 7.770(9), b 7.500(5), c 7.945(10) A, beta 91.71(3), Z 4, and contain parallel chains (-Hg-SMe-)n with neighbouring chains linked by bridging bromine atoms into parallel sheets. Each bromine is triply bridging, being coordinated to two mercury atoms in one chain, and one mercury atom in an adjacent chain. The structure of MeSHgCl appears to be isomorphous." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Structural Studies of RSHg(II) Complexes Containing (-Hg-SR-)n Rings and Chains</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Raston, C.L.</span> and <span class="person_name">White, A.H.</span> (1979) <xhtml:em>Structural Studies of RSHg(II) Complexes Containing (-Hg-SR-)n Rings and Chains.</xhtml:em> Australian Journal of Chemistry, 32 (2). pp. 311-320. ISSN 0004-9425</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2822/1/AustJ1979_2C_311.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2822/1/AustJ1979_2C_311.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />362Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="4017" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://www.publish.csiro.au/nid/51/paper/CH9790321.htm">http://www.publish.csiro.au/nid/51/paper/CH9790321.htm</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">Crystals of acetato(methanethio1ato)-gamma-picolinemercury(II), MeSHg02CMe,C6H7N (1), are monoclinic, P21/a, a 16.617(9), b 7.271(3), c 20.476(2), beta = 113.31(5), Z 8. The structure resembles that of its pyridine analogue, being based on a polymeric (-Hg-SMe-)n chain with acetate and
picoline groups coordinated at each mercury; a similar structure is found for EtSHg02CMe,C5H5N (2), monoclinic, P21/c, a 9.344(2), b 17.917(9), c 7.179(2) A, beta 106.24(3), Z 4. The structure of tetrachlorotetra(2-methylpropane-2-thiolato)di(gamma-picoline)tetramercury(11), (ButS)4CI4Hg4(C6H7N)2 (3), also resembles that of its pyridine analogue being based on an unusual tetranuclear grouping of mercury atoms linked by chloride and thiolate bridges. Crystals of (3) are monoclinic, P21/c
a 12.334(7), b 17.468(9), c 9.999(5) A, beta 91.18(4), Z 2. Crystals of MeSHgBr (4) are monolinic, P21/c, a 7.770(9), b 7.500(5), c 7.945(10) A, beta 91.71(3), Z 4, and contain parallel chains (-Hg-SMe-)n with neighbouring chains linked by bridging bromine atoms into parallel sheets. Each bromine is triply bridging, being coordinated to two mercury atoms in one chain, and one mercury atom in an adjacent chain. The structure of MeSHgCl appears to be isomorphous.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/250200.html">250000 Chemical Sciences > 250200 Inorganic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2822</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">11 Jan 2008 10:16</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">11 Jan 2008 10:16</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2822;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2822">item control page</a></p>
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